Effect of Voltage and Flow Rate Electrospinning Parameters on Polyacrylonitrile Electrospun Fibers

Malaysian Technical Universities Conference on Engineering and Technology 2017

Bakar, S.S.S.^1 ; Fong, K.C.^1 ; Eleyas, A.^1 ; Nazeri, M.F.M.^1

CEGeoGTech, School of Materials Engineering, Kompleks Pengajian Jejawi 2, Taman Muhibbah, Arau Perlis, Malaysia^1

关键词: Electrical conductivity;    Electrospinning parameters;    Electrospinning process;    Electrospun fibers;    Fibrous structures;    Polyacrylonitrile (PAN);    Polymer nanofibers;    Processing parameters;   

Others  :  https://iopscience.iop.org/article/10.1088/1757-899X/318/1/012076/pdf
DOI  :  10.1088/1757-899X/318/1/012076

来源: IOP

【 摘 要 】

Currently, electrospinning is a very famous technique and widely used for forming polymer nanofibers. In this paper, the Polyacrylonitrile (PAN) nanofibers were prepared in concentration of 10wt% with varied processing parameters that can affect the properties of PAN fiber in term of fiber diameter and electrical conductivity was presented. Voltage of 10, 15 and 20 kV with PAN flow rate of 1 electrospun PAN fibers were then undergo pyrolysis at 800°C for 30 minutes. The resultant PAN nanofibers were then analysed by SEM, XRD and four point probe test after pyrolysis process. SEM image show continuos uniform and smooth surface fibrous structure of electrospun PAN fibers with average diameter of 1.81 μm. The fiber morphology is controlled by manipulating the processing parameters of electrospinning process. The results showed that the resistance of electrospun PAN fibers decreases as the processing parameter changes by increasing the applied voltage and flow rate of electrospinning.