In Situ Gaseous Reduction (ISGR) is a technology developed by DOE for the remediation of soil waste sites contaminated with hexavalent chromium. This document presents information associated with characterization activities conducted at the 183-DR site at Hanford, which is associated with a significant groundwater contaminant plume and was formerly a water treatment facility that utilized chromate as a corrosion inhibitor. Geotechnical and chemical data were collected during the excavation of trenches and the drilling of two vadose zone boreholes to support a possible ISGR demonstration at 183-DR. Although elevated total chromium and trace levels of hexavalent chromium were identified from one of the trenches and one of the boreholes, it appears that the boreholes missed the vadose zone contaminant source responsible for the chromium groundwater plume located downgradient of the 183-DR site. Recommendations are provided, however, for future work at 183-DR that may serve to identify the source for the groundwater plume and possibly provide an opportunity for an ISGR demonstration.