科技报告详细信息
RESULTS FOR THE FIRST QUARTER 2012 TANK 50 WAC SLURRY SAMPLE: CHEMICAL AND RADIONUCLIDE CONTAMINANT RESULTS
Bannochie, C.
Savannah River Site (S.C.)
关键词: Wastes;    Sensitivity;    Sampling;    Radioisotopes;    Aqueous Solutions;   
DOI  :  10.2172/1043259
RP-ID  :  SRNL-STI-2012-00286
RP-ID  :  DE-AC09-08SR22470
RP-ID  :  1043259
美国|英语
来源: UNT Digital Library
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【 摘 要 】

This report details the chemical and radionuclide contaminant results for the characterization of the 2012 First Quarter sampling of Tank 50 for the Saltstone Waste Acceptance Criteria (WAC). Information from this characterization will be used by Waste Solidification Engineering (WSE) to support the transfer of low-level aqueous waste from Tank 50 to the Salt Feed Tank in the Saltstone Facility in Z-Area, where the waste will be immobilized. This information is also used to update the Tank 50 Waste Characterization System. The following conclusions are drawn from the analytical results provided in this memorandum: (1) The concentrations of the reported chemical and radioactive contaminants were less than their respective WAC targets or limits unless noted in this section; (2) The reported detection limit for {sup 94}Nb is above the requested limit from Reference 2 but below the estimated limit in Reference 3; (3) {sup 247}Cm and {sup 249}Cf are above the requested limits from Reference 2. however, they are below the limits established in Reference 3; (4) The reported detection limit for Norpar 13 is greater than the limit from Table 4 and Attachment 8.2 of the WAC; (5) The reported detection limit for Isopar L is greater than the limit from Table 3 of the WAC; (6) Isopar L and Norpar 13 have limited solubility in aqueous solutions making it difficult to obtain consistent and reliable sub-samples, the values reported in this report are the concentrations in the sub-sample as detected by the instrument; however, the results may not accurately represent the concentrations of the analytes in Tank 50; and (7) The low insoluble solids content increases the measurement uncertainty for insoluble species.

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