A Comparison of Microwave-Accelerated and Conventionally Heated Iodination Reactions of Some Arenes and Heteroarenes, Using ortho-Periodic Acid as the Oxidantâ€

Molecules

关键词: Oxidation;    ortho-periodic acid as oxidant;    oxidative iodination of activated arenes and heteroarenes;    diiodine;    microwave irradiation;   

DOI  :  10.3390/10020401

来源: DOAJ

【 摘 要 】

A fast and simple method for the oxidative iodination of some activated arenes and heteroarenes, either under microwave irradiation or by conventional heating, is reported, using diiodine and ortho-periodic acid as the oxidant. The reactions were carried out in hot 95% ethanol under a reflux condenser. For the microwave assisted reactions, the reaction times were always notably shortened, but the yields were nearly the same as those afforded by the conventional method.

【 授权许可】

Unknown