期刊论文详细信息
Journal of the Brazilian Chemical Society | |
Microwave-assisted clean synthesis of amides via aza-wittig reaction under solvent-free condition | |
Murugan Sathishkumar1  Sangaraiah Nagarajan1  Poovan Shanmuga Velan1  Murugan Dinesh1  Alagusundaram Ponnuswamy1  | |
[1] ,Madurai Kamaraj University School of Chemistry Department of Organic ChemistryTamilnadu,India | |
关键词: microwave; solution phase; solvent-free; amide; aza-wittig; | |
DOI : 10.1590/S0103-50532011001100007 | |
来源: SciELO | |
【 摘 要 】
A solvent-free microwave-assisted coupling of phosphazenes with acyl chlorides or carboxylic anhydrides in presence of triethylphosphite has been accomplished resulting in a clean synthesis of amides in good yields. Unlike the prevailing time-consuming solution phase methodologies employing chlorinated solvents, benzene (carcinogenic), etc, the present protocol is an eco friendly, rapid and simple approach.
【 授权许可】
CC BY
All the contents of this journal, except where otherwise noted, is licensed under a Creative Commons Attribution License
【 预 览 】
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