One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole

Molbank

Avat Arman Taherpour¹ 

[1] ¹Chemistry Department, Science Faculty, Arak Islamic Azad University, P. O. Box 38135-567, Arak, Iran ²Young Club Researchers of Arak, Islamic Azad University, P.O. Box 38135-567, Arak, Iran

关键词: Microwave assisted synthesis;    1;    3-Dipolar cycloadditions;    Benzyne intermediate;    1H-Phenanthro[9;    10-d][1;    2;    3]triazole;    1;    2;    3-Triazoles;   

DOI  :  10.3390/M577

来源: mdpi

【 摘 要 】

In this study, a fast and good yield one-pot microwave-assisted synthesis (45 seconds) of 1H-phenanthro[9,10-d][1,2,3]triazole by a 1,3-dipolar cycloaddition reaction of sodium azide and 9-bromophenanthrene in the presence of potassium tert-butoxide in DMSO as solvent is reported.

【 授权许可】

CC BY   
This is an open access article distributed under the Creative Commons Attribution License (CC BY) which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.