Synthesis and Crystal Structure of 1-(3-fluorophenyl)-3-(3,4,5- trimethoxybenzoyl)thiourea

Crystals

Aamer Saeed¹  Uzma Shaheen¹ 

[1] Department of Chemistry, Quaid-I-Azam University, Islamabad 45320, Pakistan

关键词: Synthesis;    1-(3-fluorophenyl)-3-(3;    4;    5-trimethoxybenzoyl)thiourea;    crystal structure;   

DOI  :  10.3390/cryst1020034

来源: mdpi

【 摘 要 】

The title thiourea was synthesized by reaction of 3,4,5-trimethoxybenzoyl isothiocyante with 3-fluoroaniline. The 3,4,5-trimethoxybenzoyl isothiocyante was produced in situ by reaction of 3,4,5-trimethoxybenzoyl chloride with ammonium thiocyanate in dry acetonitrile. The structure was confirmed by the spectroscopic, elemental analysis and single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P2₁/c with unit cell dimensions a = 13.0966(9), b = 16.6460(13), c = 7.8448(5), β = 106.721(5)°, V 1637.9(2) ų, Z = 4.

【 授权许可】

CC BY   
© 2011 by the authors, licensee MDPI, Basel, Switzerland.