A practical one-pot synthesis of azides directly from alcohols

Journal of Chemical Sciences

Ghanashyam Bez1¹  Lalthazuala Rokhum1¹ 

[1] Department of Chemistry, North Eastern Hill University, Shillong 793 022, India$$

关键词: Alcohol;    azide;    triphenylphosphine;    iodine;    imidazole;    chemoselective.;   

DOI  :  

来源: Indian Academy of Sciences

【 摘 要 】

Alkyl/benzyl azides can be readily synthesized in excellent yields from their corresponding alcohols by stirring a solution of sodium azide in DMSO with a thoroughly ground equimolecular mixture of triphenylphosphine, iodine and imidazole.

【 授权许可】

Unknown