期刊论文详细信息
Journal of the Brazilian Chemical Society | |
Synthesis of Modified Silica Aerogel Nanoparticles for Remediation of Vietnamese Crude Oil Spilled on Water | |
Nguyen, Hong K. D.1  | |
[1]Hanoi University of Science and Technology, Hanoi, Viet-Nam | |
关键词: aerogel; TEOS; modification; nanoparticle; silica.; | |
DOI : 10.21577/0103-5053.20180046 | |
学科分类:化学(综合) | |
来源: SciELO | |
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【 摘 要 】
New application of modified silica aerogel nanoparticles was carried out for adsorption of Vietnamese spilled crude oil obtained from Bach-Ho field. The aerogel was synthesized by atmospheric drying method without critical extraction procedure in liquefied CO2 followed by surface modification using polydimethylsiloxane precursor in n-hexane solvent. The synthesis mixture contained precise amounts of water, tetraethyl orthosilicate (TEOS), ethanol and HCl with volume ratios of 2:1:4:0.0003, respectively. The modification was established by the mixing of the as-synthesized aerogel and polydimethylsiloxane followed by calcination at 350 ºC for 4 h obtaining the surface modified aerogel. The modified aerogel was applied in the adsorption of the spilled crude oil in mild temperature and atmospheric pressure. Some techniques such as X-ray diffraction (XRD), transmission electron microscopy (TEM), Brunauer-Emmett-Teller surface area analysis (BET) and Fourier transform infrared spectroscopy (FTIR) were used for characterizing the materials.【 授权许可】
CC BY
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