Crystal structure of 5-[2-(9H-carbazol-9-yl)eth­yl]-1,3,4-oxa­diazole-2(3H)-thione

Acta Crystallographica Section E: Crystallographic Communications

El-Emary, T.I.¹  Mohamed, S.K.²  Albayati, M.R.³  Simpson, J.⁴ 

[1] Chemistry Department, Faculty of Science, Minia University, 61519 El-Minia, Egypt;Chemistry and Environmental Division, Manchester Metropolitan University, Manchester M1 5GD, England;Department of Chemistry, Faculty of Science, Assiut University, 71515 Assiut, Egypt;Department of Chemistry, University of Otago, PO Box 56, Dunedin, New Zealand

关键词: CRYSTAL STRUCTURE;    CARBAZOLE;    OXADIAZOLETHIONE;    HYDROGEN BONDS;    C-H...[PI](RING) CONTACTS;    [PI]-[PI] STACKING;   

DOI  :  10.1107/S2056989017009252

学科分类：数学（综合）

来源: International Union of Crystallography

【 摘 要 】

The title compound, C16H13N3OS, comprises an oxa­diazo­lethione ring bound to the N atom of an almostplanar carbazole ring system (r.m.s. deviation = 0.0088 Å) through an ethyl­ene chain. The oxa­diazole ring is inclined to the the carbazole ring system by 40.71 (6)°. In the crystal, N—H⋯O, N—H⋯S, C—H⋯N and C—H⋯S hydrogen bonds combine with C—H⋯π(ring) and π–π contacts to stack the mol­ecules along the b-axis direction.

【 授权许可】

CC BY