Crystal structure of 4-meth­oxy-N-[(pyrrolidin-1-yl)carbo­thio­yl]benzamide

Acta Crystallographica Section E: Crystallographic Communications

Hasbullah, S.A.¹  Heng, L.Y.³  Suhud, K.⁴  Ahmad, M.⁴  Kassim, M.B.⁴ 

[1] Natural Science Faculty, Universitas Syiah Kuala, Banda Aceh, 23111, Indonesia;Chemical Technology Program, Faculty of Science Technology, Universiti Sains Islam Malaysia, Bandar Baru Nilai, 71800 Nilai, Negeri Sembilan, Malaysia;Department of Chemistry, Mathematics &School of Chemical Sciences and Food Technology, Faculty of Science and Technology, Universiti Kebangsaan Malaysia, 43600 Selangor, Malaysia

关键词: CRYSTAL STRUCTURE;    BENZOYLTHIOUREA;    PYRROLIDINE;    THIOUREA;    BENZAMIDE;    HYDROGEN BONDING;   

DOI  :  10.1107/S2056989015003813

学科分类：数学（综合）

来源: International Union of Crystallography

【 摘 要 】

In the title compound, C13H16N2O2S, the pyrrolidine ring has a twisted conformation on the central –CH2–CH2– bond. Its mean plane is inclined to the 4-meth­oxy­benzoyl ring by 72.79 (15)°. In the crystal, mol­ecules are linked by N—H⋯O and C—H⋯O hydrogen bonds to the same O-atom acceptor, forming chains along [001]. The chains are linked via slipped parallel π–π inter­actions [inter-centroid distance = 3.7578 (13) Å], forming undulating slabs parallel to (100).

【 授权许可】

CC BY