期刊论文详细信息
Dynamic Chiropractic | |
Preparative purification of coniferyl ferulate from Angelica sinensis oil by high performance centrifugal partition chromatography | |
关键词: Angelica sinensis; coniferyl ferulate; high performance centrifugal partition chromatography; solvent extraction.; | |
DOI : | |
学科分类:医学(综合) | |
来源: MPA Media | |
【 摘 要 】
A high performance centrifugal partition chromatography (HPCPC) method was successfully developed to purify coniferyl ferulate (CF) from the extracts of commercialAngelica sinensisoil by usingn-hexane-ethyl acetate-ethanol-water (5:5:5:5, v/v) as the two-phase solvent system. The upper and lower phases of this system were used as stationary and mobile phases, respectively. The purity of coniferyl ferulate was over 98% as determined by high-performance liquid chromatography (HPLC). The structure of coniferyl ferulate was identified by MS,1H NMR and13C NMR.
【 授权许可】
Unknown
【 预 览 】
Files | Size | Format | View |
---|---|---|---|
RO201902023455542ZK.pdf | 149KB | download |