The synthesis of corncobs (zea mays) active charcoal and water hyacinth (eichornia crassipes) adsorbent to adsorb Pb(II) with it's analysis using solid-phase spectrophotometry (sps)

International Conference on Advanced Materials for Better Future 2017

Saputro, S.^1 ; Masykuri, M.^1 ; Mahardiani, L.^1 ; Kurniastuti, D.^1

Chemistry Education, Faculty of Teacher Training and Education, Sebelas Maret University, Jl. Ir. Sutami 36A, Surakarta, Central Java

57126, Indonesia^1

关键词: Absorption levels;    Combined effect;    Data collecting;    Experimental methods;    Limit of detection;    research methods;    Research results;    Solid-phase spectrophotometry;   

Others  :  https://iopscience.iop.org/article/10.1088/1757-899X/333/1/012054/pdf
DOI  :  10.1088/1757-899X/333/1/012054

来源: IOP

【 摘 要 】

This research aim to examine the effect of the combination between corncobs and water hyacinth to adsorb lead (II), the most effective combination have determined by compared the ratio of corncobs adsorbent and water hyacinth to the increasing adsorption of the Pb(II), prove the effectiveness of the solid-phase spectrophotometry (sps) to determine the levels of Pb(II) as the result of the corncobs active charcoal adsorption and water hyacinth in the level of μg/L. The research method used is experimental method. The data collecting technique is carried out by several stages, which are carbonization using muffle furnace at a temperature of 350°C for 1.5 hours, activation of the corncobs charcoal and water hyacinth using HCl 1M and HCl 5M activator, contacting the adsorbent of corncobs active charcoal and water hyacinth with liquid waste simulation of Pb(II) using variation of corncobns and water hyacinth, 1:0; 0:1; 1:1; 2:1; 1:2, analysis of Pb(II) using an sps, characterization of corncobs active charcoal adsorbent and water hyacinth using FTIR. Research results show that the combined effect of activated charcoal corncobs and water hyacinth can increase the ability of the adsorbent to absorb Pb(II), the optimum adsorbent mass ratio of 1:1 with the absorption level of 90.33%, SPS is an effective method to analyze the decreasing level of Pb(II) as the adsorbtion result of the corncobs active charcoal and water hyacinth in the level of μg/L, with the limit of detection (LOD) of 0.06 μg/L.