Determination of Betaine in Lycii Cortex by Capillary Electrophoresis

1st International Conference on Frontiers of Materials Synthesis and Processing

材料科学;化学

Peng, Xuewei^1 ; Liu, Haixing^1

Chemistry and Chemical and Environmental Engineering College, Weifang University, Weifang

261061, China^1

关键词: Borax solution;    Buffer solutions;    Constant voltage;    Correlation coefficient;    High performance capillary electrophoresis;    Pressure time;   

Others  :  https://iopscience.iop.org/article/10.1088/1757-899X/274/1/012073/pdf
DOI  :  10.1088/1757-899X/274/1/012073

学科分类：材料科学（综合）

来源: IOP

【 摘 要 】

This paper presents the determination of betaine content in Lycii Cortex by high performance capillary electrophoresis (HPCE) method. The borax solution was chosen as buffer solution, and its concentration was 40 mmol at a constant voltage of 20kV and injecting pressure time of 10s at 14°C. Linearity was kept in the concent ration range of 0.0113∼1.45mg of betaine with correlation coefficient of 0.9. The content of betaine in Lycii Cortex was 61.9 mg/g (RSD = 13.4%) (n = 7). The recovery was in the range of 86.6%-118.1% (n=4). This method is specific, simple and rapid and accurate, which is suitable for the detection of the content of betaine in Lycii Cortex.