Influence of synthesis conditions on the crystallinity of hydroxyapatite obtained by chemical deposition

International Conference and Youth Scientific School on "Materials and Technologies of New Generations in Modern Materials Science"

Toropkov, N.E.^1 ; Vereshchagin, V.I.^1 ; Petrovskaya, T.S.^1,2 ; Antonkin, N.S.^1

Tomsk Polytechnic University, 30 Lenin ave., Tomsk

634050, Russia^1

Skolkovo Institute of Science and Technology, Moscow, Russia^2

关键词: Carbonate-substituted hydroxyapatite;    Chemical deposition;    Crystallinities;    Hydroxyapatite synthesis;    Nanocrystalline phase;    Reaction medium;    Reaction temperature;    Synthesis conditions;   

Others  :  https://iopscience.iop.org/article/10.1088/1757-899X/156/1/012038/pdf
DOI  :  10.1088/1757-899X/156/1/012038

来源: IOP

【 摘 要 】

The hydroxyapatite synthesis on a variety of substrates under various conditions was studied. It was shown that the increase in the temperature of the reaction medium increases the amount of nanocrystalline phase with an average crystallite size of 25 nm. Studies revealed that in addition to the pure hydroxyapatite, β-Ca3(PO4)2 along with calcium carbonates and carbonate-substituted hydroxyapatites were formed. A significant increase in phase crystallinity during the heating of reactants up to the reaction temperature was shown.