2nd international Tropical Renewable Energy Conference 2017 | |
Effect of electrolyte type on the morphology and crystallinity of TiO2 nanotubes from Ti-6Al-4V anodization | |
Gibran, Khalil^1 ; Ibadurrahman, Muhammad^1 ; Slamet^1 | |
Chemical Engineering Department, Faculty of Engineering, Universitas Indonesia, Depok | |
16424, Indonesia^1 | |
关键词: Anatase crystals; Anodizing methods; Anodizing process; Antibacterial properties; Crystallinities; Electrolyte solutions; Ethylene glycol solutions; Influential factors; | |
Others : https://iopscience.iop.org/article/10.1088/1755-1315/105/1/012038/pdf DOI : 10.1088/1755-1315/105/1/012038 |
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来源: IOP | |
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【 摘 要 】
A good biocompatibility material such as Ti-6Al-4V is neededfor a dental application.However,Ti-6Al-4V has no antibacterial properties. Therefore Ti-6Al-4V is modified using anodizing methods to improve its anti-bacterial properties. One of the most influential factors in the anodizing process is the type of electrolyte solution. The influence of electrolyte solution based on glycerol and ethylene glycol to morphology and crystallinity of TiO2nanotubes is studied. Smoothing and chemical polishing was performed against the Ti-4Al-6V plate. Then, the anodizing process for each plate in glycerol and ethylene glycol solution was done for 2 hours and 50 volts. Calcination was carried out for 3 hours at a temperature 500°C. FESEM-EDX and XRD were employed to analyze the surface morphology and crystallinity of TiO2nanotubes. Viscosity of the electrolyte solution influenced surfacemorphology. Calcination process influenced crystallinity of TiO2nanotubes.The average tube diameter and thickness from glycerolelectrolyte solution was 135.45 nm and 26.27 nm, while ethylene glycol was 68.52 nm and 35.62 nm respectively. The size of anatase crystal was 34.95 nm for glycerol and 44.77 nm for ethylene glycol.
【 预 览 】
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Effect of electrolyte type on the morphology and crystallinity of TiO2 nanotubes from Ti-6Al-4V anodization | 643KB | ![]() |