Development of extraction and cleanup approaches for PFASs analysis in fish tissue by HPLC-MS/MS technique

Arctic Biomonitoring

Sorokin, A.V.^1 ; Ovcharenko, V.V.^1 ; Turbabina, K.A.^1 ; Kozhushkevich, A.I.^1 ; Kalantaenko, A.M.^1 ; Komarov, A.A.^1

Russian State Center for Quality and Standardization of Veterinary Drugs and Feed (VGNKI), Moscow

123022, Russia^1

关键词: Cleanup approach;    Current status;    Environmental distribution;    Fish tissue;    HPLC-MS/MS;    Ppb levels;    Sample preparation;    Stockholm;   

Others  :  https://iopscience.iop.org/article/10.1088/1755-1315/263/1/012060/pdf
DOI  :  10.1088/1755-1315/263/1/012060

来源: IOP

【 摘 要 】

The history of PFASs emergence and current status in the context of the Stockholm Convention on POPs, their environmental distribution and toxicity are discussed. Various approaches to PFASs analysis in fish tissues are discussed. An original method of sample preparation is described, which allows quantitative PFASs determination at 0.2100 ppb levels.