Synthesis, structural and morphological property of a novel Pd/g-CN nano composite for gas sensing application

4th International Conference on Structural NanoComposites

Ibrahim, A.^1^2^3 ; Memon, U.B.^1^2^3 ; Kumar, J. Praveen^5 ; Duttagupta, S.P.^2 ; Raman, R. K. Singh^3^4 ; Sarkar, A.^5 ; Pendharkar, G.^7 ; Tatiparti, S.S.V.^6

IITB-Monash Research Academy, Indian Institute of Technology Bombay, India^1

Department of Electrical Engineering, Indian Institute of Technology Bombay, India^2

Department of Chemical Engineering, Monash University, Australia^3

Department of Mechanical and Aerospace Engineering, Monash University, Australia^4

Department of Chemical Engineering, Indian Institute of Technology Bombay, India^5

Department of Energy Science and Engineering, Indian Institute of Technology Bombay, India^6

Department of Electrical and Computer Systems Engineering, Monash University, Australia^7

关键词: EDS analysis;    Energy dispersive spectroscopies (EDS);    Gas sensing applications;    Graphitic carbon nitrides;    Material characterizations;    Muffle furnaces;    Palladium nano particles;    Structural and morphological properties;   

Others  :  https://iopscience.iop.org/article/10.1088/1757-899X/499/1/012003/pdf
DOI  :  10.1088/1757-899X/499/1/012003

来源: IOP

【 摘 要 】

In this paper graphitic carbon nitride (g-CN) was synthesized using urea as a precursor at temperature 550 0C in a muffle furnace. Palladium Nano-particles were introduced in the graphic carbon nitride matrix by fairly new chemical sol-gel process followed by filtering and drying. Material characterization such as X-Ray Diffraction (XRD), Scanning electron microscopy (SEM), Transmission electron microscopy (TEM) and Energy-dispersive spectroscopy (EDS) were performed. XRD indicates the formation of polycrystalline material. SEM and TEM analysis indicate the uniform Palladium nanostructures impregnated g-CN matrix. EDS analysis justifies the presence of all the elements.