Separation of Corn Fiber and Conversion to Fuels and Chemicals Phase II: Pilot-scale Operation

Abbas, Charles ; Beery, Kyle ; Orth, Rick ; Zacher, Alan

关键词: ANIMAL FEEDS;    ETHANOL;    FERMENTATION;    FIBERS;    GLUCOSE;    GLYCOLS;    MOLASSES;    OLIGOSACCHARIDES;    PROPYLENE;    PURIFICATION;    RESIDUES;    SACCHARIDES;    SOLVENTS;    STILLAGE;    XYLOSE;    YEASTS Corn Fiber;    Ethanol;    biofuels;    corn oil;    wet mill;    phytosterols;   

DOI  :  10.2172/916996
RP-ID  :  GO13147-Final
PID  :  OSTI ID: 916996
Others  :  TRN: US200821%%340

学科分类：燃料技术

美国|英语

来源: SciTech Connect

【 摘 要 】

The purpose of the Department of Energy (DOE)-supported corn fiber conversion project, “Separation of Corn Fiber and Conversion to Fuels and Chemicals Phase II: Pilot-scale Operation” is to develop and demonstrate an integrated, economical process for the separation of corn fiber into its principal components to produce higher value-added fuel (ethanol and biodiesel), nutraceuticals (phytosterols), chemicals (polyols), and animal feed (corn fiber molasses). This project has successfully demonstrated the corn fiber conversion process on the pilot scale, and ensured that the process will integrate well into existing ADM corn wet-mills. This process involves hydrolyzing the corn fiber to solubilize 50% of the corn fiber as oligosaccharides and soluble protein. The solubilized fiber is removed and the remaining fiber residue is solvent extracted to remove the corn fiber oil, which contains valuable phytosterols. The extracted oil is refined to separate the phytosterols and the remaining oil is converted to biodiesel. The de-oiled fiber is enzymatically hydrolyzed and remixed with the soluble oligosaccharides in a fermentation vessel where it is fermented by a recombinant yeast, which is capable of fermenting the glucose and xylose to produce ethanol. The fermentation broth is distilled to remove the ethanol. The stillage is centrifuged to separate the yeast cell mass from the soluble components. The yeast cell mass is sold as a high-protein yeast cream and the remaining sugars in the stillage can be purified to produce a feedstock for catalytic conversion of the sugars to polyols (mainly ethylene glycol and propylene glycol) if desirable. The remaining materials from the purification step and any materials remaining after catalytic conversion are concentrated and sold as a corn fiber molasses. Additional high-value products are being investigated for the use of the corn fiber as a dietary fiber sources.