Advanced Materials and Processes for High Energy Resolution Room Temperature Gamma Ray Spectrometers

Douglas S. McGregor

关键词: GAMMA SPECTROMETERS;    TELLURIUM;    PURIFICATION;    VACUUM DISTILLATION;    ZONE MELTING;    CADMIUM;    ZINC;    MANGANESE;    FABRICATION;   

DOI  :  10.2172/925851
RP-ID  :  DOE/ID/14725
PID  :  OSTI ID: 925851
Others  :  TRN: US0802499

美国|英语

来源: SciTech Connect

【 摘 要 】

A significant amount of progress has been achieved in the development of the novel vacuum distillation method described in the proposal. The process for the purification of Te was fully developed and characterized in a series of trials. The purification effect was confirmed with GDMS sample analysis and indicates the process yields very high purity Te metal. Results of this initial process study have been submitted for publication in the Proceedings of the SPIE and will be presented on August 28, 2007 at the SPIE Optics and Photonics 2007 conference in San Diego, CA. Concurrent to the development of the Te process, processes for the purification of Cd, Zn, and Mn have also progressed. The development of the processes for Cd and Zn are nearly complete, while the development of the process for Mn is still in its infancy. It is expected that a full characterization of the Cd process will be completed within the next quarter, followed by Zn. Parallel to those characterization studies, efforts will be made to further develop the Mn purification process. Zone melting work for Te and Cd has also been efforted as per the project work schedule. Initial trials have been completed and the processes developed. Characterization of the results will be completed within the first fiscal year. Finally, an apparatus for the zone refinement of Cd, Zn, and Mn has been constructed and initial trials are set to begin shortly.