Verification Of The Defense Waste Processing Facility's (DWPF) Process Digestion Methods For The Sludge Batch 8 Qualification Sample

Click, D. R. ; Edwards, T. B. ; Wiedenman, B. J. ; Brown, L. W.

关键词: method development;    analytical process;    SB8;    waste compliance;   

DOI  :  10.2172/1076959
RP-ID  :  SRNL-STI--2013-00096
PID  :  OSTI ID: 1076959
Others  :  TRN: US1300145

学科分类：核能源与工程

美国|英语

来源: SciTech Connect

【 摘 要 】

This report contains the results and comparison of data generated from inductively coupled plasma ??? atomic emission spectroscopy (ICP-AES) analysis of Aqua Regia (AR), Sodium Peroxide/Sodium Hydroxide Fusion Dissolution (PF) and Cold Chem (CC) method digestions and Cold Vapor Atomic Absorption analysis of Hg digestions from the DWPF Hg digestion method of Sludge Batch 8 (SB8) Sludge Receipt and Adjustment Tank (SRAT) Receipt and SB8 SRAT Product samples. The SB8 SRAT Receipt and SB8 SRAT Product samples were prepared in the SRNL Shielded Cells, and the SRAT Receipt material is representative of the sludge that constitutes the SB8 Batch or qualification composition. This is the sludge in Tank 51 that is to be transferred into Tank 40, which will contain the heel of Sludge Batch 7b (SB7b), to form the SB8 Blend composition.