Transient liquid phase bonding of titanium to aluminium nitride

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING

卷:495

Article; Proceedings Paper

Dezellus, O.¹  Andrieux, J.¹  Bosselet, F.¹  Sacerdote-Peronnet, M.¹  Baffie, T.²  Hodaj, E.³  Eustathopoulos, N.³  Viala, J. C.¹ 

[1] Univ Lyon 1, CNRS, LMI, F-69622 Villeurbanne, France

[2] CEA, LITEN DTH LTH, F-38054 Grenoble 9, France

[3] CNRS, ENSEEG, SIMAP, F-38420 St Martin Dheres, France

关键词: Transient liquid phase bonding;    Isothermal solidification;    Metal to ceramic brazing;    Ag-Cu alloy;    Experimental study;    Interfacial reactivity;   

DOI  :  10.1016/j.msea.2007.10.104

来源: Elsevier

【 摘 要 】

Titanium has been successfully joined to aluminium nitride AlN at a temperature as low as 795 degrees C, using Ag-Cu Cusil(R) commercial braze alloy. While reactive wetting and spreading proceeds at the AlN/braze alloy interface, chemical interactions develop at the titanium side rendering possible isothermal solidification of the joint. The determining factor in the solidification process is the fast formation of TiCu4 crystals by heterogeneous nucleation and growth in the liquid phase. As a consequence, the braze alloy is depleted in Cu and solid Ag precipitates. After annealing, the re-melting temperature of the resulting joint can be increased up to about 910 degrees C which is nearly 130 degrees C higher than the melting point of the starting braze alloy. (C) 2008 Elsevier B.V. All rights reserved.

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