Crystal structure of N′-[bis(ethylsulfanyl)methylidene]-2-hydroxy-4-methoxybenzohydrazide

Acta Crystallographica Section E: Crystallographic Communications

Manoj K. Bharty¹  Rahul Chaurasia¹  Sanyucta Kumari¹  Paras Nath¹  Sushil K. Gupta² 

[1] Department of Chemistry, Banaras Hindu University, Varanasi 221 005, India;School of Studies in Chemistry, Jiwaji University, Gwalior 474 011, India;

关键词: crystal structure;    dithiocarbazate;    hydrogen bonding;    ester;   

DOI  :  10.1107/S2056989015021271

来源: DOAJ

【 摘 要 】

In the title compound, C13H18N2O3S2, the amide group is in the plane of the benzoyl ring with a C—N—N—C torsion angle of 177.63 (12)°. The two dithioate groups are in an anti conformation [torsion angles = 173.68 (8) and −9.98 (10)°]. An intramolecular N—H...O hydrogen bond is observed. In the crystal, an O—H...O hydrogen bond and a weak C—H...O contact involving the same acceptor atom generate an S(6) ring motif and give rise to chains along [010].

【 授权许可】

Unknown