Other compounds isolated from Simira glaziovii and the ¹H and 13C NMR chemical shift assignments of new 1-epi-castanopsol

Química Nova

Ivo J. Curcino Vieira¹  Marcelo F. de Araújo²  Mário G. de Carvalho²  Raimundo Braz-Filho² 

[1] Universidade Estadual do Norte Fluminense;Universidade Federal Rural do Rio de Janeiro;

关键词: ¹H and 13C-NMR;    1-epi-castanopsol;    Simira glaziovii;   

DOI  :  10.1590/S0100-40422012001100019

来源: DOAJ

【 摘 要 】

A new triterpene, 1-epi-castanopsol, besides eleven known compounds: sitosterol, stigmasterol, campesterol, lupeol, lupenone, simirane B, syringaresinol, scopoletin, isofraxidin, 6,7,8-trimethoxycoumarin and harman, were isolated from the wood of Simira glaziovii. The structures of the known compounds were defined by 1D, 2D ¹H, 13C NMR spectra data analyses and comparison with literature data. The detailed spectral data analyses allowed the definition of the structure of the new 1-epi isomer of castanopsol and performance of ¹H and 13C NMR chemical shift assignments.

【 授权许可】

Unknown