Microwave Sintering of Ti6Al4V: Optimization of Processing Parameters for Maximal Tensile Strength and Minimal Pore Size

Metals

Dilpreet Singh¹  Dinesh Kalyanasundaram¹  Abhishek Rana¹  PulakMohan Pandey²  Pawan Sharma² 

[1] Centre for Biomedical Engineering, Indian Institute of Technology Delhi, New Delhi 110016, India;Department of Mechanical Engineering, Indian Institute of Technology Delhi, New Delhi 110016, India;

关键词: microwave sintering;    Ti6Al4V;    tensile strength;    pore;    computed tomography;    RSM;    additive manufacturing;   

DOI  :  10.3390/met8121086

来源: DOAJ

【 摘 要 】

Pressureless sintering is a powder metallurgical process wherein the powder particles are sintered without the aid of any compressive force. Though this additive manufacturing process is economical, the strength of the component is undermined due to the presence of pores; the elimination of which is a challenge. In this work, the optimal process parameters for the pressureless microwave sintering of a grade 5 titanium alloy that yields higher tensile strength and minimum sizes of pores were obtained. The three process parameters (sintering temperature, heating rate, and holding time) were experimented at five different levels using the design of experiments (DOE). Post sintering, the tensile strength was assessed as per ASTM standard B925-15, while the pore size was evaluated, non-destructively, using micro-computed tomography (µ-CT). The optimal process parameters that yielded minimum size pores were: sintering temperature—1293 °C, heating rate—6.65 °C/min; and holding time—72 min.

【 授权许可】

Unknown