Facile solvothermal synthesis of bimetallic CoMoS2 and NiMoS2 nanospheres

Green Processing and Synthesis

Rodríguez-Ramos Inmaculada¹  Guerrero-Ruíz Antonio¹  Gallegos-Suárez Esteban¹  Chafik Tarik²  Mateos-Pedrero Cecilia³ 

[1] ;Laboratory LGCVR, UAE/L01FST, Faculty of Sciences and Techniques, University Abdelmalek Essaadi, B.P. 416 Tangier, Morocco;Laboratory for Process Engineering, Environment, Biotechnology and Energy, Faculdade de Engenharia da Universidade do Porto Rua Roberto Frias, s/n4200-465 Porto, Portugal;

关键词: comos2;    mos2;    nanospheres;    nimos2;    solvothermal synthesis;   

DOI  :  10.1515/gps-2015-0017

来源: DOAJ

【 摘 要 】

Bimetallic nickel or cobalt molybdenum disulfide (MMoS2, M=Ni or Co) nanospheres, with a diameter ranging between 450 nm and 1 μm, have been successfully synthesized using a mild solvothermal method. The obtained nanomaterials have been comprehensively characterized using transmission electron microscopy (TEM), high resolution TEM (HRTEM), energy-dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetry analysis (TGA), X-ray photoelectron spectroscopy (XPS) and temperature-programmed reduction (TPR).

【 授权许可】

Unknown