A Novel Fabrication of Spherical Fe50Ni50 Alloy Powders via in-Situ De-Wetting of Liquid Solid Interface

Crystals

Wei Zhong¹  Xueyin Song¹  Chenglong Lei² 

[1] Collaborative Innovation Center of Advanced Microstructures, National Laboratory of Solid State Microstructures and Jiangsu Provincial Laboratory for NanoTechnology, Nanjing University, Nanjing 210093, China;College of Engineering and Applied Science, Nanjing University, Nanjing 210093, China;

关键词: spherical Fe-Ni powders;    de-wetting;    alumina;    liquid-solid interface;    magnetic properties;   

DOI  :  10.3390/cryst9070325

来源: DOAJ

【 摘 要 】

Spherical Fe₅₀Ni₅₀ alloy powders were fabricated via a novel route based on in-situ interface de-wetting between liquid Fe-Ni alloy and alumina. The obtained Fe₅₀Ni₅₀ alloy particles exhibit very good spherical shape according to SEM images. Furthermore, the cross-sectional SEM images show that there are no pores and bulk inclusions in the internal region of the spherical particles. The XRD results show a trace amount of the impurity alumina phase appearing in taenite phase. The size distribution agreed well with the SEM observation confirms that the alumina powders successfully segregated pre-alloy powders. As an incidental benefit, the surface alumina particles were treated as the electrical insulation coatings. The magnetic character shows that spherical Fe₅₀Ni₅₀ powders exhibit a good soft magnetic property even though with a slightly decreasing of saturation magnetization due to non-magnetic coatings. Our strategies provide a method to in-situ fabricate insulation coated Fe-Ni spherical alloy powders as magnetic powder core.

【 授权许可】

Unknown