期刊论文详细信息
Green Processing and Synthesis | |
Iodination of industrially important aromatic compounds using N-iodosuccinimide by grinding method | |
article | |
Vivek Sharma1  Priyanka Srivastava2  Santosh Kumar Bhardwaj2  D.D. Agarwal2  | |
[1] Department of Chemistry, Baba Farid College;Department of Industrial Chemistry, Jiwaji University | |
关键词: aromatic; catalysis; iodoarenes; regiospecific; | |
DOI : 10.1515/gps-2017-0072 | |
来源: De Gruyter | |
【 摘 要 】
Iodination of various industrially and pharmaceutically important substituted aromatics has been achieved using N-iodosuccinimide (NIS) in solid state by grinding at room temperature. This method provides several advantages such as short reaction time (5–8 min), high yields (94–99%), and nonhazardous and simple work-up procedure. High gas chromatography (GC) purity (95–99.9%) suggests that the reaction is highly selective. Substrates which are sensitive to oxidation, viz aniline and phenols are iodinated smoothly in high yield.
【 授权许可】
CC BY
【 预 览 】
Files | Size | Format | View |
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RO202107200001626ZK.pdf | 3479KB | download |