Processing of high performance composites based on peek by aqueous suspension prepregging

Materials Research

Liliana Burakowski Nohara²  Michelle Leali Costa²  Mauro Angelo Alves¹  Marta Ferreira Koyama Takahashi¹  Evandro Luís Nohara¹  Mirabel Cerqueira Rezende¹ 

[1] ,Universidade Estadual Paulista Faculty of Engineering Department of Materials and TechnologyGuaratinguetá SP ,Brazil

关键词: carbon fiber;    interphase;    thermoplastic polymer;   

DOI  :  10.1590/S1516-14392010000200020

来源: SciELO

【 摘 要 】

The use of polyamic acid (PAA) precursor as interphase in polymer composites is one of the many applications of polyimides (PIs). In this work, composites based on poly(ether-ether-ketone) (PEEK) and carbon fibers were prepared using two manufacturing techniques for thermoplastic composites: hot compression molding, and aqueous polymeric suspension prepregging using PIs as interphase. Two PAAs were synthesized and used as interphases: 3,3'-4,4'-benzophenonetetracarboxylic dianhydride/oxydianiline (BTDA/ODA) and pyromellitic dianhydride/oxydianiline (PMDA/ODA). The PAA/PI systems were analyzed by differential scanning calorimetry (DSC), thermogravimetry (TGA), Fourier transform infrared spectroscopy (FTIR) and nuclear magnetic resonance (NMR). Results from these analyses confirmed the synthesis of these compounds. Aqueous polymeric suspension prepregging was more efficient than hot compression molding when the PMDA/ODA PAA/PI interphase was used; also, the interlaminar shear strength of composites produced using this technique was 14.5% higher than the one produced using hot compression molding.

【 授权许可】

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