期刊论文详细信息
Journal of the Brazilian Chemical Society
Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometry
Sandra Jorge2  Carlos E. S Coelho1  Francisco Radler De Aquino-neto2 
[1] ,Universidade Federal do Rio de Janeiro Instituto de Química Rio de Janeiro RJ ,Brazil
关键词: fluid inclusions;    petroleum;    mass spectrometry;    hydrocarbons;    quartz;   
DOI  :  10.1590/S0103-50532011000300005
来源: SciELO
PDF
【 摘 要 】

A new tool has been increasingly used in organic geochemistry; it is the application of fluid inclusions hosted in minerals, mainly quartz, from rock samples recovered in basin wells. In this paper we develop a new practical screening method to identify the presence of petroleum in fluid inclusions from siliciclastic and carbonatic minerals. The method is called detection of petroleum inclusions and allows analyzing the presence of volatiles in oil fluid inclusions extracted by online crushing from cuttings samples. This method offers the advantage of working with solid samples, as a micro-scaled sealed vessel (MSSV) system. Moreover it is simple, relatively fast and presents a satisfactory reproducibility. For the successful analysis it is essential to carefully control the analytical procedures, including the cleaning of samples and blank runs. Results were compared with previously reported methods

【 授权许可】

CC BY   
 All the contents of this journal, except where otherwise noted, is licensed under a Creative Commons Attribution License

【 预 览 】
附件列表
Files Size Format View
RO202005130106434ZK.pdf 1293KB PDF download
  文献评价指标  
  下载次数:4次 浏览次数:14次