O uso de aparelhos de micro-ondas domésticos em aulas experimentais de química orgânica: nitração de salicilaldeído

Química Nova

Eurídes Francisco Teixeira²  Ana Paula Bernardo Dos Santos²  Renato Saldanha Bastos²  Angelo C. Pinto²  Arthur Eugen Kümmerle¹  Roberto Rodrigues Coelho¹ 

[1] ,Universidade Federal do Rio de Janeiro Cidade Universitária Centro de TecnologiaRio de Janeiro RJ ,Brasil

关键词: microwave;    nitration;    salicylaldehyde;   

DOI  :  10.1590/S0100-40422010000700032

来源: SciELO

【 摘 要 】

The use of microwave in chemistry has known benefits over conventional heating methods, e.g. reduced reaction times, chemical yield improvement and the possibility if reducing or eliminating the use of organic solvents. We describe herein a procedure for the nitration of salicylaldehyde in water using a domestic microwave oven, which can be used as an experiment in the undergraduate chemistry laboratory. The experiment involves safe and rapid preparation and identification of the position isomers by thin layer chromatography and 1H NMR, or by their melting points.

【 授权许可】

CC BY-NC   
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