Uso de frascos de polipropileno descartáveis no pré-tratamento de amostras de água para determinação de chumbo, cobre e mercúrio por voltametria de onda quadrada

Química Nova

Eduardo M. Richter¹  Claudimir L. Do Lago¹  Lúcio Angnes¹ 

[1] ,Universidade de São Paulo Instituto de Química Departamento de Química FundamentalSão Paulo SP ,Brasil

关键词: sample pretreatment;    water analysis;    polypropylene vials;   

DOI  :  10.1590/S0100-40422006000400039

来源: SciELO

【 摘 要 】

In this work a simple and versatile procedure is described for treating water samples using small polypropylene (PP) vials (4 mL) for determining heavy metals by square wave voltammetry (SWV). This procedure involves treatment with nitric acid (0.2 mol L-1) and boiling in a water-bath (~ 100 ºC). This process is completed after one hour and allows the pretreatment of several samples simultaneously. The accuracy was estimated using addition/recovery studies and certified water sample analysis, yielding an agreement near to 100%.

【 授权许可】

CC BY-NC   
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