The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation†

Molecules

Ellis Benjamin¹ 

[1] Department of Chemistry and Physics, Arkansas State University, State University, AR 72467, USA E-mail:

关键词: Hydroxylamine∙HCl;    unsubstituted cyclic imides;    DMAP;    microwaves;   

DOI  :  10.3390/molecules13010157

来源: mdpi

【 摘 要 】

Unsubstituted cyclic imides were synthesized from a series of cyclic anhydrides, hydroxylamine hydrochloride (NH₂OH∙HCl), and 4-N,N-dimethylamino-pyridine (DMAP, base catalyst) under microwave irradiation in monomode and multimode microwaves. This novel microwave synthesis produced high yields of the unsubstituted cyclic imides for both the monomode (61 - 81%) and multimode (84 - 97%) microwaves.

【 授权许可】

Unknown   
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