N,N'-1,2-Phenylenebis[4-(chloromethyl)benzamide]

Molbank

Jürgen Bachl¹ 

[1] ¹Institut für Organische Chemie, Universität Regensburg, Universitätsstr 31, 93040 Regensburg, Germany ²ICMA, CSIC-Universidad de Zaragoza, Pedro Cerbuna 12, 50009 Zaragoza, Spain

关键词: o-phenylenediamine;    benzamide;    nucleophilic acyl substitution;   

DOI  :  10.3390/M705

来源: mdpi

【 摘 要 】

N,N'-1,2-Phenylenebis[4-(chloromethyl)benzamide] (3) was obtained in 61% yield by nucleophilic acyl substitution of 4-(chloromethyl)benzoyl chloride (2) with 1,2-phenylenediamine (1) under basic conditions. The title compound was characterized by FT-IR, ¹H NMR, ¹³C NMR, low- and high-resolution EI-MS, and melting point.

【 授权许可】

CC BY   
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