Synthesis and Crystal Structure of 3-(4-Methoxyphenyl)-2-thioxo-2,3-dihydroquinazolin-4(1H)-one

Crystals

Aamer Saeed¹  Shams ul Mahmood¹ 

[1] Department of Chemistry, Quaid-I-Azam University, Islamabad 45320, Pakistan

关键词: quinazolinone;    3-aryl-2-thioxo-2;    3-dihydroquinazolin-4(1H)-ones;    synthesis;   

DOI  :  10.3390/cryst1030171

来源: mdpi

【 摘 要 】

Synthesis of the title compound from 4-methoxyaniline was accomplished in three steps. The structure was supported by spectroscopic data and unambiguously confirmed by single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P2₁ with unit cell dimensions a = 9.9349(8), b = 6.3377(5), c = 10.5783(10) Å, β = 97.752(3)°, V = 659.97(10) ų, Z = 2.

【 授权许可】

CC BY   
© 2011 by the authors, licensee MDPI, Basel, Switzerland.