Synthesis and NMR Spectral Studies of the 7-C60-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine

Molecules

Zhi Zhou¹ 

[1] College of Chemical Engineering, Nanjing Forestry University, Nanjing 210037, China

关键词: 7-C 60-adduct of N;    N-(tetrachlorophthaloyl) dehydroabietylamine;    ¹H-NMR;    ¹³C-NMR;    2D NMR;    C₁ symmetric structure;   

DOI  :  10.3390/molecules17044209

来源: mdpi

【 摘 要 】

The 7-C₆₀-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The ¹H-NMR and ¹³C-NMR resonance signals of the new compound are unambiguously assigned by using homo- and heteronuclear 2D NMR spectroscopic techniques such as COSY, ROESY, HSQC and HMBC. The C₁ symmetric structure with 6,6-junction of compound was determined.

【 授权许可】

CC BY   
© 2012 by the authors; licensee MDPI, Basel, Switzerland.