3-Chloro-5-(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

Molbank

Heraklidia A. Ioannidou¹ 

[1] Department of Chemistry, University of Cyprus, P.O. Box 20537, 1678 Nicosia, Cyprus

关键词: 1;    2;    6-thiadiazines;    thiophenes;    heterocycles;    oligomers;   

DOI  :  10.3390/M782

来源: mdpi

【 摘 要 】

3-Chloro-5-trifluoromethanesulfonate-4H-1,2,6-thiadiazin-4-one 3 reacts with (4-dodecylthiophen-2-yl)trimethylstannane 5 (1 equiv.) in the presence of Pd(Ph₃P)₂Cl₂ (5 mol%) in benzene at ca. 20 °C for 5 h to give 3-chloro-5-(4-dodecylthien-2-yl)-1,2,6-thiadiazinone 6 in 87% yield.

【 授权许可】

CC BY   
This is an open access article distributed under the Creative Commons Attribution License (CC BY) which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.