A Novel Fluoride Route for the Synthesis of Aluminosilicate Nanotubes

Nanomaterials

Atika Chemmi²  Jocelyne Brendlé¹  Claire Marichal² 

[1] Equipe Matériaux à Porosité Controlée (MPC), Institut de Science des Matériaux de Mulhouse (IS2M), CNRS UMR 7361, Université de Haute Alsace (UHA), ENSCMu, 3b rue Alfred Werner, 68093 Mulhouse Cedex, France;

关键词: aluminosilicate nanotube;    imogolite;    fluoride route;    synthesis;   

DOI  :  10.3390/nano3010117

来源: mdpi

【 摘 要 】

In this work we present a novel method for synthesis of aluminosilicate nanotubes: the fluoride route. F-containing imogolite (F-IMO) exhibits an improved crystallization rate and improved yield. The structure of F-IMO was investigated and compared with F-free imogolite (IMO) by means of X-ray diffraction (XRD) and Fourier transformed infrared spectroscopy (FTIR) confirming imogolite structure. Solid state nuclear magnetic resonance (NMR) analyses show an increased crystallization rate for F-IMO and confirm the incorporation of fluorine ion in the structure.

【 授权许可】

CC BY   
© 2013 by the authors; licensee MDPI, Basel, Switzerland.