10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene

Molbank

Kosuke Yamamoto¹  Ryota Nakamae¹  Hiroshi Suemune¹ 

[1] Graduate School of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku,Fukuoka 812-8582, Japan

关键词: azulene-fused helicene;    homocoupling reaction;    ammonium persulfate;   

DOI  :  10.3390/M843

来源: mdpi

【 摘 要 】

The title compound was prepared by the regioselective homocoupling of10-methoxyazuleno[2,1-c]phenanthrene in the presence of ammonium persulfate. The structure of the synthesized compound was assigned on the basis of its ¹H-NMR, FT-IR, and mass spectral data. Its crystal structure and electrochemical properties are also reported.

【 授权许可】

CC BY   
This is an open access article distributed under the Creative Commons Attribution License (CC BY) which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.