Hydrolysis of Azadirachta indica oil using subcritical water and determination of triacylglycerides and fat acids by HT-HRGC-FID and HRGC-MS

Química Nova

Pinto, Jair Sebastião da Silva¹  Lanças, Fernando Mauro¹  Universidade de São Paulo, São Carlos, Brasil¹ 

关键词: Neem oil;    subcritical water;    Green Analytical Chemistry (GAC).;   

DOI  :  10.1590/S0100-40422010000200029

学科分类：化学（综合）

来源: Sociedade Brasileira de Quimica

【 摘 要 】

The development of modern analytical tools plays an important role in quality control. The main purpose of this study was to explore the use of subcritical water as a versatile analytical tool, employed simultaneously as a reagent and solvent, as well as the application of high temperature-high resolution gas chromatography (HT-HRGC) to develop a procedure for the analysis of triacylglycerides and fatty acids in Azadirachta indica A. Juss. (Neem) oil without the need for solvents, chemical reagents, or catalytic agents. The developed method presented satisfactory results and is in agreement with the concepts of Green Analytical Chemistry (GAC).

【 授权许可】

Unknown