Synthesis and characterization of CdS and CdSe nanoparticles prepared from novel intramolecularly stabilized single-source precursors

Journal of Chemical Sciences

Karuppasamy Kandasamy²  Harkesh B Singh1²  Shailendra K Kulshreshtha¹ 

[1]Novel Materials and Structural Chemistry Division, Bhabha Atomic Research Center, Mumbai 400 085$$

[2]Department of Chemistry, Indian Institute of Technology Bombay, Powai, Mumbai 400 076$$

关键词: Nanoparticle;    CdSe;    CdS;    TEM;    XRD;    SEM;    hexagonal phase.;   

DOI  :  

来源: Indian Academy of Sciences

【 摘 要 】

In this note we describe the synthesis of cadmium sulphide and selenide nanoparticles from the corresponding novel single source precursors, M[E(Ox)]2 [E = S (1), Se (2); M = Cd; Ox = 2-(4,4-dimethyl-2-oxazolinyl)benzene] by thermolysing in tri-𝑛-octylphosphine oxide (TOPO) at 280°C, and their characterization by X-ray powder diffraction (XRD), transmission electron microscope (TEM) and scanning electron microscope (SEM) studies.

【 授权许可】

Unknown