Sequencing of peracetylated oligosaccharides by rotating‐frame nuclear Overhauser enhancement spectroscopy

FEBS Letters

Bruntz, Renate¹  Dabrowski, Janusz²  Ejchart, Andrzej²  Egge, Heinz¹ 

[1] Institut für Physiologische Chemie, Universität Bonn, Nussallee 11, D-5300 Bonn, FRG;Max-Planck-Institut für Medizinische Forschung, Jahnstrasse 29, D-6900 Heidelberg FRG

关键词: Peracetylated oligosaccharide;    Oligosaccharide sequencing;    NMR;    rotating frame 1H-;    HOHAHA;    homonuclear Hartmann-Hahn spectroscopy;    NOE;    nuclear Overhauser enhancement;    NOESY;    two-dimensional NOE spectroscopy;    ROESY;    rotating-frame NOE;    TOCSY;    total correlation spectroscopy;   

DOI  :  10.1016/0014-5793(89)80288-1

学科分类：生物化学/生物物理

来源: John Wiley & Sons Ltd.

【 摘 要 】

A combination of two-dimensional total correlation spectroscopy (TOCSY) and rotating-frame nuclear Overhauser enhancement spectroscopy (ROESY) is suggested as the optimum strategy for determining the primary structure of peracetylated oligosaccharides.

【 授权许可】

Unknown