Bulletin of the Korean chemical society | |
Synthesis of Platinum Nanostructures Using Seeding Method | |
You Jung Song1  Jong Min Lee1  Do Hyung Kim1  Sang Beom Han1  Kyung Won Park1  Jy Yeon Kim1  | |
关键词: Platinum; Hexapod; Shape control; Seeding method; | |
DOI : | |
学科分类:化学(综合) | |
来源: Korean Chemical Society | |
【 摘 要 】
We report Pt hexapod nanoparticles with 6.4 ~ 9.7 nm in size by a polyol process in the presence of PVP as a stabilizer and additive as a kinetic controller. The structure and morphology of Pt nanostructures are confirmed by field-emission transmission electron microscopy. The morphological control over platinum nanoparticles is achieved by varying the amount of seeds in the polyol process, where platinum precursor is reduced by ethylene glycol to form Pt nanoparticle at 150 oC. As volume ratio between precursor-solution and seed-solution is increased from 10 to 50, the shape of Pt nanostructures is evolved from small seeds to tripod and hexapod. In addition, the size-controlled platinum hexapod nanostructures are successfully obtained using seeding method.
【 授权许可】
Unknown
【 预 览 】
Files | Size | Format | View |
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RO201912010241244ZK.pdf | 2407KB | download |