Effect of nanocrystalline surface of substrate on microstructure and wetting of PEO coatings

Bulletin of materials science

H R Masiha¹  H R Bagheri¹  M Gheytani¹  M Aliofkhazraei¹  T Shahrabi¹  A Sabour Rouhaghdam¹ 

[1] Department of Materials Science, Faculty of Engineering, Tarbiat Modares University, Tehran, P.O. Box: 14115-143, Iran$$Department of Materials Science, Faculty of Engineering, Tarbiat Modares University, Tehran, P.O. Box: 14115-143, IranDepartment of Materials Science, Faculty of Engineering, Tarbiat Modares University, Tehran, P.O. Box: 14115-143, Iran$$

关键词: Aluminium;    nanocrystallization;    nanoparticles;    plasma electrolyte oxidation;    surface mechanical attrition treatment.;   

DOI  :  

学科分类：材料工程

来源: Indian Academy of Sciences

【 摘 要 】

In this research, effect of surface mechanical attrition treatment (SMAT) was studied on characteristics of the coatings formed using plasma electrolyte oxidation (PEO) on AA1230 aluminium. To do so, first, the samples were coated with and without SMAT pre-process. Coating by PEO method was carried out in two phosphate-based and silicate-based suspensions of silicon nitride nanoparticles for 10 min. Next, to study the distribution of the nanoparticles and elements inside the coating, surface morphology of the samples was examined using scanning electron microscopy and energy dispersive spectroscopy. In addition, wettability test was performed on all samples using the deionized water. Also, droplet expansion manner on the porous oxide coating surface and its relation with fine structure of the coating was investigated. The results indicated that samples coated in silicate-based electrolyte have a relatively rougher microstructure as compared to samples coated in phosphate-based electrolyte. The average surface pores area percentage of the samples coated in silicate-based electrolytes was 13.9% greater than that of samples coated in phosphate-based electrolyte. Moreover, the average height to diameter (h/d) value obtained from wettability test for samples coated in silicate-based electrolyte was 13.3% greater than that of phosphate-based electrolyte.

【 授权许可】

Unknown