Preparation of PbSe nanoparticles by electron beam irradiation method

Bulletin of materials science

Minghong Wu¹  Zheng Jiao¹  Tiebing Liu¹  Yanyan Liu¹  Chao Wu¹  Zhen Li¹ 

[1] Institute of Nanochemistry and Nanobiology, School of Environmental and Chemical Engineering, Shanghai University, Shanghai 200444, P.R. China$$Institute of Nanochemistry and Nanobiology, School of Environmental and Chemical Engineering, Shanghai University, Shanghai 200444, P.R. ChinaInstitute of Nanochemistry and Nanobiology, School of Environmental and Chemical Engineering, Shanghai University, Shanghai 200444, P.R. China$$

关键词: Lead selenide;    nanoparticle;    electron beam;    irradiation.;   

DOI  :  

学科分类：材料工程

来源: Indian Academy of Sciences

【 摘 要 】

A novel method has been developed by electron beam irradiation to prepare PbSe nanoparticles. 2 MeV 10mA GJ-2-II electronic accelerator was used as radiation source. Nanocrystalline PbSe was prepared rapidly at room temperature under atmospheric pressure without any kind of toxic reagents. The structure and morphology of prepared PbSe nanoparticles were analysed by X-ray diffraction, transmission electron microscope and atomic force microscope. The results indicated that the obtained materials were cubic nanocrystalline PbSe with an average grain size of 30 nm. The optical properties of prepared PbSe nanocrystalline were characterized by using photoluminescence spectroscopy. The possible mechanism of the PbSe grain growth by electron beam irradiation method is proposed.

【 授权许可】

Unknown