Bulletin of materials science | |
Synthesis of size-controlled Bi particles by electrochemical deposition | |
S Sampath1  H C Thejaswini1  C N Tharamani1  | |
[1] Department of Inorganic and Physical Chemistry, Indian Institute of Science, Bangalore 560 012, India$$Department of Inorganic and Physical Chemistry, Indian Institute of Science, Bangalore 560 012, IndiaDepartment of Inorganic and Physical Chemistry, Indian Institute of Science, Bangalore 560 012, India$$ | |
关键词: Bismuth nanoparticles; electrodeposition; SEM; TEM; XPS.; | |
DOI : | |
学科分类:材料工程 | |
来源: Indian Academy of Sciences | |
【 摘 要 】
Small sized bismuth particles are prepared by an electrochemical method using a triple voltage pulse technique. The bath composition and electrochemical parameters are optimized to yield monodisperse particles. The particles have been characterized by scanning electron microscopy, transmission electron microscopy, energy dispersive X-ray analysis, X-ray photoelectron spectroscopy, UV-visible spectroscopy and X-ray diffraction technique. The particles, as deposited, are highly crystalline in nature and the particle size and shape get tuned depending on the conditions of deposition.
【 授权许可】
Unknown
【 预 览 】
Files | Size | Format | View |
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RO201912010228945ZK.pdf | 1310KB | download |