Synthesis, X-ray structure and N�?�H…O interactions in 1,3-diphenyl-urea

Bulletin of materials science

Rajnikant¹  Dinesh¹  Kamni¹  M B Deshmukh² 

[1] PG Department of Physics, University of Jammu, Jammu Tawi 180 006, India$$PG Department of Physics, University of Jammu, Jammu Tawi 180 006, IndiaPG Department of Physics, University of Jammu, Jammu Tawi 180 006, India$$;Department of Chemistry, Shivaji University, Kolhapur 416 004, India$$Department of Chemistry, Shivaji University, Kolhapur 416 004, IndiaDepartment of Chemistry, Shivaji University, Kolhapur 416 004, India$$

关键词: Alkaloids;    X-ray structure;    diffractometer;    hydrogen bond.;   

DOI  :  

学科分类：材料工程

来源: Indian Academy of Sciences

【 摘 要 】

The synthesis, X-ray structure and role of intermolecular interactions have been studied in case of 1,3-diphenyl-urea, owing to its medicinal importance. The compound crystallizes in orthorhombic crystal system (space group, 𝑃ð�?��?�ð�?��?2₁) with unit cell parameters, ð‘�? = 9.118(3), ð‘�? = 10.558(2), ð‘�? = 11.780(3) Ã�? and ð‘�? = 4. The structure has been solved by direct methods and refined to a final ð‘�??-value of 0.0316. The oxygen atom of the carbonyl group is responsible for the existence of two Nâ€�?�H…O intermolecular interactions.

【 授权许可】

Unknown