Microwave promoted a green protocol for solvent free synthesis of 1,5-benzothiazepine and [1,3,4]-thiadiazepine derivatives incorporating thiophene moiety

Green Chemistry Letters and Reviews

Tamer S. Saleh¹ 

关键词: 1;    5-Benzothiazepine;    1;    3;    4-thiadiazepine;    solvent free;    microwave irradiations;   

DOI  :  10.1080/17518253.2011.628953

学科分类：化学（综合）

来源: Taylor & Francis

【 摘 要 】

An efficient and environmentally benign procedure is developed for the synthesis of 1,5-benzothiazepine and 1,2,4-triazolo[3,4-b][1,3,4] thiadiazepine derivatives in good to excellent yield under solvent-free microwave irradiations using silica sulfuric acid or basic alumina respectively as solid supports.

【 授权许可】

Unknown