Bulletin of Materials Science | |
Gel–sol synthesis and aging effect on highly crystalline anatase nanopowder | |
关键词: Gel–sol; anatase; titania; nanoparticles; aging.; | |
学科分类:材料工程 | |
来源: Indian Academy of Sciences | |
【 摘 要 】
Highly crystalline TiO2 anatase nanoparticles were synthesized via gel–sol method by using titanium isopropoxide and triethanolamine. The products were characterized by X-ray diffraction, transmission electron microscopy, thermogravimetric/differential thermal analysis and nitrogen gas absorption methods. The particle size ranged from 7 to 24 nm having specific surface area of 64 to 220 m2/g. Selective Ti(OH)4 gel specifications and hydrothermal test conditions resulted in thermodynamically-stable phase-formation. Aging at 130°C for 4 h resulted in particle size of 7 nm; while at 130 and 160°C for 12 h resulted in 12 and 21 nm, respectively.
【 授权许可】
CC BY
【 预 览 】
Files | Size | Format | View |
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RO201902182245671ZK.pdf | 316KB | download |