Monomer conversion of composite dental resins photoactivated by a halogen lamp and a LED: a FT-Raman spectroscopy study

Quimica nova

Pinheiro, Antonio L. B.¹  Zampieri, Marcelo²  Soares, Luís Eduardo Silva³  Martin, Airton Abrahão³  Rocha, Rick³ 

[1] Universidade Federal da Bahia, Salvador;Universidade Federal de São Carlos, São Carlos;Universidade do Vale do Paraíba, São José dos Campos

关键词: composites;    degree of conversion;    FT-Raman spectroscopy.;   

DOI  :  10.1590/S0100-40422005000200012

学科分类：化学（综合）

来源: Sociedade Brasileira de Quimica

【 摘 要 】

Eighteen circular blocks of resins cured eitherby a LED or a halogen lamp (20, 40 and 60 s), had their top (T) and bottom (B)surfaces studied using a FT-Raman spectrometer. Systematic changes in the intensityof the methacrylate C=C stretching mode at 1638 cm-1 as a functionof exposure duration were observed. The calculated degree of conversion (DC)ranged from 45.0% (B) to 52.0% (T) and from 49.0% (B) to 55.0% (T) for the LEDand halogen lamp, respectively. LED and halogen light produced similar DC valueswith 40 and 60 s of irradiation.

【 授权许可】

CC BY